Nitrogen Gas Dehydration and Drying Solution

Industry Pain Points

  • Trace Moisture Endangering Process Safety: Residual moisture in nitrogen (≥10ppm) causes wafer oxidation in semiconductor manufacturing, with a single loss reaching 5 million RMB; in the chemical industry, it triggers catalyst poisoning, and the replacement cost exceeds 2 million RMB per time.
  • Limitations of Traditional Dehydration Technologies: Freeze drying can only achieve a dew point of +3℃; adsorptive desiccants suffer severe pulverization under high pressure (≥5MPa), shortening their service life from 5 years to 6 months.
  • Severe Energy Waste: The energy consumption for regeneration of conventional PSA drying ranges from 0.2 to 0.3 kWh/Nm³, and the annual electricity consumption of a 10,000-scale air separation system exceeds 8 million RMB.
  • Poor Adaptability to Complex Working Conditions: Nitrogen pressure fluctuations (0.5-10MPa), oil content (0.1-5ppm), and acidic gases (CO₂/H₂S) lead to equipment corrosion and adsorbent poisoning.

SYSTEM OVERVIEW

Yipu Nitrogen Dehydration System adopts the technology chain of “cryogenic pre-dehydration – high-pressure adsorption – heatless regeneration” to achieve:

  • Process Safety: Completely eliminates the risks of catalyst poisoning and product oxidation caused by moisture.
  • Energy Consumption Revolution: The comprehensive energy consumption is 70% lower than the industry standard, reducing carbon emissions by 2,000 tons annually (for 10,000-scale air separation systems).
  • Intelligent Protection: AI dynamically optimizes the adsorption/regeneration sequence, with an availability rate of ≥99.9%.

Technology Evolution

  • Launched a helium-compatible version in 2024, suitable for rare gas recovery in the semiconductor industry.
  • This solution is a core equipment for high-end manufacturing and energy industries to achieve independent and controllable ultra-pure gas.

Solution Approach

Yipu Nitrogen Dehydration and Drying Solution

ModuleTechnical HighlightsPerformance Parameters
Cryogenic UnitR404A/R23 cascade refrigeration, explosion-proof Ex dⅡCT4Pre-cooling dew point -20℃, energy consumption ≤ 0.07 kWh/Nm³
High-Pressure Adsorption TowerCarbon fiber-wound shell, pressure resistance 15MPaOutlet dew point -70℃ @ 10MPa
Oil Contamination TreatmentCatalytic oxidation oil removal module (Pt/TiO₂)Residual oil ≤ 0.001 ppm, no consumables
Heatless RegenerationNitrogen reverse purge regeneration, zero external energy supplyRegeneration energy consumption ≤ 0.01 kWh/Nm³
Intelligent MonitoringIoT platform for real-time early warning of adsorbent saturationService life prediction error ≤ 3 days

Applicable Scenarios

  • Electronic-grade high-purity nitrogen (≤0.1ppm H₂O)
  • Chemical high-pressure nitrogen sealing systems (5-10MPa)
  • Protective gas for lithium battery pole piece drying
  • Aerospace fuel pipeline purging

Technical Principles

Yipu Three-Stage Deep Dehydration Process

  1. High-Efficiency Pre-Cooling (Stage 1): The -40℃ cryogenic heat exchanger cools nitrogen from 40℃ to -20℃, removing 80% of free water (dew point -20℃), with a refrigerant COP ≥ 4.0.
  2. Anti-Pollution Adsorption (Stage 2): Composite adsorption bed:
    • Upper layer: Oil-repellent activated alumina intercepts oil mist (residual oil ≤ 0.001 ppm)
    • Lower layer: 3A-N2 molecular sieve achieves a dew point of -70℃ under 10MPa high pressure
  3. Intelligent Regeneration (Stage 3): Adopts nitrogen self-circulation regeneration (heatless regeneration technology), saving 90% more energy than traditional electric heating.
  4. Precision Control: Laser dew point meter (accuracy ±0.5℃) + AI algorithm dynamically adjusts the adsorption cycle.

CORE ADVANTAGE

Advantage CategoryDescription
Customized on DemandMeets special working conditions; provides professional non-standard customization
Low CostAdopts cyclic regeneration process; significantly reduces usage costs
High StabilityDouble-tower structure with small pressure fluctuation; low noise and continuous gas supply
Fully Automatic OperationEasy to operate, reducing labor input; improves efficiency
High SafetyPresets multi-level safety protection measures; supports automatic alarm
Low Failure RateMaintains low failure rate after 10,000 hours of operation; nearly maintenance-free durability

TECHNICAL STRENGTH

Leading Adsorption Dehydration Technology

  • Uses high-performance molecular sieve adsorbents with high water absorption capacity and resistance to acidic gas (H₂S/CO₂) corrosion, ensuring deep dehydration with a dew point ≤ -70℃.
  • Features an original hot nitrogen regeneration process, reducing energy consumption by 30% compared to traditional electric heating regeneration, and integrates a waste heat recovery system to significantly improve energy efficiency.

Modular and Customized Design Capability

  • Core equipment adopts modular prefabrication, supporting rapid deployment (installation cycle shortened by 50%) and adapting to diverse scenarios such as offshore platforms, onshore gas fields, and LNG pre-treatment.
  • Can customize single-tower, double-tower, or multi-tower parallel systems according to customer needs, with a treatment capacity ranging from 10,000 to 1,000,000 Nm³/d, flexibly matching gas fields of different scales.

Intelligent Control and Remote Operation & Maintenance

  • Equipped with a PLC+IoT intelligent control system to monitor key parameters such as pressure, temperature, and dew point in real time, supporting fault early warning and automatic adjustment.
  • Optimizes the adsorption-regeneration cycle through cloud-based big data analysis, extending the service life of molecular sieves and reducing operation and maintenance costs by 10%-15%.

Energy-Saving and Environmental Protection Technology

  • Features zero-emission design for regenerated tail gas, complying with EU CE, US EPA, and other environmental standards.
  • Energy consumption is 25%-40% lower than that of traditional Triethylene Glycol (TEG) dehydration systems, helping customers achieve carbon emission reduction goals.

Long-Cycle Operation Reliability

  • Molecular sieves adopt anti-pulverization coating technology, with a service life of over 5 years, reducing replacement frequency.
  • Key components (such as valves and instruments) are selected from international first-tier brands (e.g., Siemens, Emerson), with a Mean Time Between Failures (MTBF) of over 100,000 hours.

Strong R&D and Engineering Experience

  • Possesses 19+ patents for dehydration technology and software copyrights; the R&D team is led by doctors and cooperates in-depth with universities and colleges.
  • Has over 1,000 successful cases worldwide, covering extreme working conditions such as high-sulfur gas fields in the Middle East and low-temperature environments in the Arctic.

Product Advantage Comparison

IndicatorYipu SystemFreeze-TypeTraditional PSACompetitor Adsorption-Type
Dew Point-70℃ (at 10MPa)+3℃-40℃ (atmospheric pressure)-60℃ (service life only 2 years)
Residual Oil Content≤0.001 ppm≤1 ppmNo oil removal function≤0.01 ppm
Energy Consumption0.08 kWh/Nm³ (comprehensive)0.1 kWh/Nm³0.25 kWh/Nm³0.18 kWh/Nm³
Pressure Adaptability0.5-10MPa lossless operationRequires pressure stabilization to 0.7MPaOnly applicable for 0.5-0.8MPa1-6MPa
Service Life8 years (molecular sieve)No consumables5 years (frequent replacement required)3 years

Typical Case

Project Name: Ultra-High Purity Nitrogen Project in a 12-Inch Wafer Fab

Working Conditions

  • Treatment Capacity: 8,000 Nm³/h, pressure 5MPa
  • Requirements: Dew point ≤ -65℃, oil content ≤ 0.001 ppm

Results

  • Stable dew point of -68℃, oil content of 0.0003 ppm
  • Wafer oxidation defect rate reduced from 3% to 0.02%

Economic Benefits

  • Annual electricity cost savings of 4.2 million RMB
  • Reduced annual wafer scrap losses by 180 million RMB